DIPROPYL SULFATE
- Name DIPROPYL SULFATE
- CAS 598-03-8
- Purity 99%
Product Details
Buy Good Quality DIPROPYL SULFATE 598-03-8 with a minimum purity of 99%
- Molecular Formula: C6H14 O2 S
- Molecular Weight: 150.242
- Appearance/Colour: WHITE TO OFF-WHITE CRYSTALLINE LOW MELTING SOLID
- Vapor Pressure: 0.0343mmHg at 25°C
- Melting Point: 27-31 °C
- Refractive Index: n20/D 1.413
- Boiling Point: 266°Cat760mmHg
- Flash Point: 125.8°C
- PSA： 42.52000
- Density: 1.01g/cm3
- LogP: 2.30200
DIPROPYL SULFATE(Cas 598-03-8) Usage
|
Synthesis Reference(s) |
The Journal of Organic Chemistry, 26, p. 1331, 1961 DOI: 10.1021/jo01063a632 |
InChI:InChI=1/C6H14O4S/c1-3-5-9-11(7,8)10-6-4-2/h3-6H2,1-2H3
598-03-8 Relevant articles
Synthesis, spectral characterization, SC-XRD, HSA, DFT and catalytic activity of novel dioxovanadium(V) complex with aminobenzohydrazone Schiff base ligand: An experimental and theoretical approach
Ashfaq, Muhammad,Behjatmanesh-Ardakani, Reza,Fallah-Mehrjardi, Mehdi,Kargar, Hadi,Munawar, Khurram Shahzad,Tahir, Muhammad Nawaz
, (2021/07/28)
A new dioxovanadium(V) complex was prepa...
Synthesis, spectra (FT-IR, NMR) investigations, DFT, FMO, MEP, NBO analysis and catalytic activity of MoO2(VI) complex with ONO tridentate hydrazone Schiff base ligand
Behjatmanesh-Ardakani, Reza,Fallah-Mehrjardi, Mehdi,Kargar, Hadi,Munawar, Khurram Shahzad
, (2021/08/16)
A new dioxomolybdenum(VI) complex has be...
Magneli-type tungsten oxide nanorods as catalysts for the selective oxidation of organic sulfides
D?ren, René,Hartmann, Jens,Leibauer, Benjamin,Panth?fer, Martin,Mondeshki, Mihail,Tremel, Wolfgang
, p. 14027 - 14037 (2021/10/19)
Selective oxidation of thioethers is an ...
Synthesis method of sulfone compound
-
Paragraph 0030-0034, (2020/01/25)
The invention discloses a synthesis meth...
598-03-8 Process route
-
-
111-47-7
propyl sulfide
-
-
4253-91-2
dipropyl sulfoxide
-
-
598-03-8
propyl sulfone
| Conditions | Yield |
|---|---|
|
With
chlorine dioxide;
In
ethyl acetate;
at 20 ℃;
for 1h;
|
95%
2% |
|
With
nano-sized mesoporous sodium iron hydroxyphosphate supported gold; dihydrogen peroxide;
In
methanol; water;
at 60 ℃;
for 0.5h;
Green chemistry;
|
95.6%
|
|
With
aluminium trichloride; butyltriphenylphosphonium dichromate;
In
acetonitrile;
for 0.0125h;
microwave irradiation;
|
85%
|
|
With
iron(II) acetylacetonate; oxygen;
at 100 ℃;
for 6h;
under 15001.5 Torr;
chemoselective reaction;
Autoclave;
|
83%
6 %Chromat. |
|
With
1H-imidazole; tetra-n-butylammonium hydrogen monopersulfate;
In
dichloromethane;
at 25 ℃;
for 0.0333333h;
chemoselective reaction;
|
82%
18% |
|
With
[5,10,15,20-tetrakis(2,3,4,5,6-pentafluorophenyl)porphyrinato]platinum(II); iodosylbenzene;
In
dichloromethane;
at 20 ℃;
for 0.5h;
Catalytic behavior;
|
80%
12% |
|
With
aluminium trichloride; 3-carboxypyridinium chlorochromate;
In
acetonitrile;
for 0.0055h;
microwave irradiation;
|
79%
|
|
With
chlorine dioxide;
at 20 ℃;
for 0.5h;
|
95 % Chromat.
2 % Chromat. |
|
With
dihydrogen peroxide;
phosphomolybdic acid hydrate;
In
acetonitrile;
at 29.85 ℃;
for 3h;
Product distribution;
Mechanism;
other sulphides, other catalysts: H4PVMo11O40, H5PV2Mo10O40, H6PV3Mo9O40, H5PV2W10O40, H3PMo6W6O40, K7PTi2W10O40;
|
|
|
With
dihydrogen peroxide;
phosphomolybdic acid hydrate;
In
acetonitrile;
at 29.85 ℃;
for 3h;
Yield given;
Yields of byproduct given;
other catalysts: H4PVMo11O40, H5PV2Mo10O40, H6PV3Mo9O40, H5PV2W10O40, H3PMo6W6O40, K7PTi2W10O40;
|
|
|
With
dihydrogen peroxide;
H6PV3Mo9O40;
In
acetonitrile;
at 29.85 ℃;
for 3h;
Yield given;
Yields of byproduct given;
other catalysts: H3PMo12O40, H4PVMo11O40, H5PV2Mo10O40, H5PV2W10O40, H3PMo6W6O40, K7PTi2W10O40;
|
|
|
With
[N,N'-bis(2-oxo-3,5-di-chlorophenylmethyl)-N,N'-bis(1,3-benzodioxol-5-ylmethyl)ethylenediamine]Ti(OiPr)2; dihydrogen peroxide;
In
methanol; water;
at 20 ℃;
for 0.5h;
chemoselective reaction;
Inert atmosphere;
|
|
|
With
C38H26N6NiS2(2+)*2NO3(1-); dihydrogen peroxide;
In
water; acetonitrile;
at 20 ℃;
|
|
|
With
3-chloro-benzenecarboperoxoic acid;
In
chloroform-d1;
|
|
|
With
1H-imidazole; tetra-n-butylammonium hydrogen monopersulfate;
In
ethanol; dichloromethane;
at 25 ℃;
for 0.0333333h;
chemoselective reaction;
|
79 %Chromat.
21 %Chromat. |
|
With
1H-imidazole; [(2-(2'-hydroxyphenyl)-5,6-dihydro-1,3-oxazine)2Mn(OAc)]; urea hydrogen peroxide adduct;
In
methanol; dichloromethane;
at 20 ℃;
for 0.0833333h;
|
|
|
With
tert.-butylhydroperoxide; C48H68O96V29(7-)*H(1+)*6K(1+)*26H2O;
In
dichloromethane;
at 25 ℃;
for 0.5h;
|
|
|
With
dihydrogen peroxide;
In
acetonitrile;
at 35 ℃;
for 0.0833333h;
|
|
|
With
dihydrogen peroxide; C100H124O18Ti4*4C2H3N;
In
acetonitrile;
at 60 ℃;
for 2h;
Reagent/catalyst;
|
|
|
With
tungsten oxide; dihydrogen peroxide;
In
d(4)-methanol;
for 0.5h;
Time;
|
-
-
111-47-7
propyl sulfide
-
-
598-03-8
propyl sulfone
| Conditions | Yield |
|---|---|
|
With
tert.-butylhydroperoxide; aluminum tri-tert-butoxide;
In
benzene;
|
100%
|
|
With
tert.-butylhydroperoxide; [Mo2(O)4{[2,2'-(1,3-phenylene)bis(4,5-dihydrooxazole-4,2-diyl)]dimethanol}(acac)2];
In
1,2-dichloro-ethane;
for 0.5h;
Reflux;
|
100%
|
|
With
sodium periodate; ruthenium-carbon composite;
In
water;
at 20 ℃;
for 2h;
|
100%
|
|
With
dihydrogen peroxide;
In
water;
at 20 ℃;
for 10h;
|
99%
|
|
With
Oxone; kaolin;
In
dichloromethane;
for 4h;
Ambient temperature;
|
98%
|
|
With
dihydrogen peroxide; urea; trifluoroacetic anhydride;
In
acetonitrile;
for 0.5h;
Ambient temperature;
|
98%
|
|
With
tert.-butylhydroperoxide; aluminum tri-tert-butoxide;
In
benzene;
at 20 ℃;
for 1h;
|
98%
|
|
With
N-methylpyrrolidine-2-one hydrotribromide; dihydrogen peroxide;
In
water; acetonitrile;
at 80 ℃;
for 0.0833333h;
|
98%
|
|
With
dihydrogen peroxide;
In
nitromethane;
at 20 ℃;
for 2.5h;
|
98%
|
|
With
potassium sulfate; potassium hydrogensulfate; potassium peroxomonosulfate; wet-montmorillonite;
In
dichloromethane;
for 2h;
Ambient temperature;
|
97%
|
|
With
formic acid; dihydrogen peroxide; urea;
for 1h;
Ambient temperature;
|
96%
|
|
With
aluminium trichloride; 3-carboxypyridinium chlorochromate;
In
acetonitrile;
for 0.0166667h;
microwave irradiation;
|
95%
|
|
With
N,N'-dibenzyl-N,N,N',N'-tetramethylethylenediammonium bis(permanganate); acetic acid;
In
acetonitrile;
at 20 ℃;
for 0.0333333h;
|
95%
|
|
With
1,3,5-trichloro-2,4,6-triazine; dihydrogen peroxide;
In
water; acetonitrile;
at 20 ℃;
for 0.5h;
chemoselective reaction;
|
95%
|
|
With
O40PW12(3-)*3C14H16NO3S(1+); dihydrogen peroxide;
In
water;
at 20 ℃;
for 0.333333h;
Green chemistry;
|
95%
|
|
With
(pyridinium)H3PMo11VO40; dihydrogen peroxide;
In
water; acetonitrile;
at 40 ℃;
for 2.5h;
|
95%
|
|
With
dihydrogen peroxide;
In
n-heptane; water;
at 20 ℃;
for 0.166667h;
|
95%
|
|
With
dihydrogen peroxide;
In
ethanol; hexane; water;
at 60 ℃;
for 0.0833333h;
|
95%
|
|
With
aluminium trichloride; butyltriphenylphosphonium dichromate;
In
acetonitrile;
for 0.025h;
microwave irradiation;
|
94%
|
|
With
tert.-butylhydroperoxide;
In
benzene;
for 4.5h;
|
94%
|
|
With
dihydrogen peroxide;
In
1,2-dichloro-ethane;
for 0.2h;
Reflux;
|
94%
|
|
With
potassium permanganate;
In
acetonitrile;
at 20 ℃;
for 6h;
|
92%
|
|
With
potassium permanganate;
manganese(II) sulfate;
at 20 ℃;
for 1.1h;
|
92%
|
|
With
[bis(acetoxy)iodo]benzene; toluene-4-sulfonic acid;
In
water;
at 80 ℃;
for 24h;
|
89%
|
|
With
sodium hypochlorite;
In
acetonitrile;
for 1h;
Ambient temperature;
|
86%
|
|
With
manganese(IV) oxide; potassium permanganate;
In
dichloromethane;
at 20 ℃;
for 4.5h;
|
86%
|
|
With
dihydrogen peroxide; C16H16N3O5V;
In
ethanol; water;
for 0.5h;
Reflux;
|
85%
|
|
With
chlorine dioxide;
In
water;
at 50 ℃;
for 10h;
|
82%
|
|
With
phthalic anhydride; urea;
In
acetonitrile;
for 0.5h;
Ambient temperature;
other sulfides;
|
|
|
With
permanganate(VII) ion;
|
|
|
With
dihydrogen peroxide; acetic acid;
|
|
|
With
sodium hypochlorite;
|
|
|
With
phthalic anhydride; urea;
In
acetonitrile;
for 0.5h;
Ambient temperature;
|
|
|
With
peroxyhexanoyl nitrate;
In
pentane;
at 0 ℃;
for 0.25h;
Yield given;
|
|
|
Multi-step reaction
with
2
steps
1: 3,3-dimethyldioxirane / acetone / 19.84 °C
2: 3,3-dimethyldioxirane / acetone / 19.84 °C
With
3,3-dimethyldioxirane;
In
acetone;
|
|
|
With
3-chloro-benzenecarboperoxoic acid;
In
chloroform-d1;
|
|
|
With
oxone; water;
at 60 ℃;
for 12h;
chemoselective reaction;
|
|
|
With
(dimethyl dioctadecylammonium)7[PW11O39]; dihydrogen peroxide;
In
1,4-dioxane; water;
at 59.84 ℃;
for 0.5h;
|
|
|
With
Na10K22[Zr24O22(OH)10(H2O)2(W2O10H)2(GeW9O34)4(GeW8O31)2]*85H2O; dihydrogen peroxide;
In
dodecane; acetonitrile;
at 25 ℃;
for 1h;
Sealed tube;
|
|
|
With
bis(N-isopropylsalicylaldiminato)oxovanadium(IV); dihydrogen peroxide;
In
neat (no solvent);
at 45 ℃;
for 1.66667h;
Green chemistry;
|
|
|
With
dihydrogen peroxide;
In
water;
at 24.84 ℃;
for 3h;
Green chemistry;
|
99 %Chromat.
|
|
With
O40SiV2W10(6-)*2H(1+)*4C21H46NO3S(1+); dihydrogen peroxide;
In
water;
at 24.84 ℃;
for 2h;
Green chemistry;
|
|
|
With
5Na(1+)*10K(1+)*17H(1+)*54H2O*Sc6Sb2W6O19(22+)*6SbW9O33(9-); dihydrogen peroxide;
In
acetonitrile;
at 80 ℃;
for 3h;
Reagent/catalyst;
|
|
|
With
dihydrogen peroxide;
In
acetonitrile;
at 25 ℃;
for 0.333333h;
Catalytic behavior;
Reflux;
|
|
|
With
γ-1,2-H2SiV2W10O40(4-); dihydrogen peroxide; N-Hexadecyl-N,N-dimethyl-3-ammonio-1-propanesulfonate;
In
water;
at 20 ℃;
for 2h;
|
|
|
With
4K(1+)*37H2O*6C2H2O5P(3-)*5H(1+)*3Tb(3+)*2Mo8O24; dihydrogen peroxide;
In
acetonitrile;
at 50 ℃;
for 1h;
|
|
|
With
[TMA]4H8[Na5Sb3(Sb2Mo12O57)]*17H2O; dihydrogen peroxide;
In
water;
at 25 ℃;
for 3h;
chemoselective reaction;
|
|
|
With
14C2H7N*2C2H3O2(1-)*22H2O*14H(1+)*Ru4As4W40O140(12-); dihydrogen peroxide;
In
acetonitrile;
at 50 ℃;
for 0.833333h;
|
|
|
With
4C23H50NO3S(1+)*[HPV2W10O40](4-); dihydrogen peroxide;
In
water;
at 24.84 ℃;
for 6h;
Catalytic behavior;
Green chemistry;
|
|
|
With
dihydrogen peroxide;
In
acetonitrile;
at 20 ℃;
for 0.283333h;
|
|
|
With
sodium periodate;
In
water; acetonitrile;
at 20 ℃;
for 0.5h;
|
100 %Chromat.
|
|
With
dihydrogen peroxide; C100H132O14Ti4;
In
acetonitrile;
at 60 ℃;
for 2h;
Reagent/catalyst;
|
|
|
With
dihydrogen peroxide; C17H19MoN3O7;
In
ethanol; water;
Reflux;
Green chemistry;
|
598-03-8 Upstream products
-
16841-48-8
diallyl sulfone
-
111-47-7
propyl sulfide
-
4253-91-2
dipropyl sulfoxide
-
38405-93-5
Di(1-propenyl) sulfone
598-03-8 Downstream products
-
187737-37-7
propene
-
55109-28-9
propane-1-sulfinic acid
-
1159172-45-8
1-phenyl-2-(propylsulfonyl)butan-1-ol
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